N-(4-甲氧基苯亚甲基)苯胺合成路线 （共 83 条）
反应条件
in diethyl ether
Heating;
参考文献
Satsumabayashi,S. et al.
Synthesis, 1977 , p. 881 - 883
反应条件
bis(cyclopentadienyl)titanium dichloride; samarium in tetrahydrofuran
4 h; Heating;
参考文献
Liao, Puhong; Huang, You; Zhang, Yongmin
Synthetic Communications, 1997 , vol. 27, # 9 p. 1483 - 1486
反应条件
1: With ytterbium; methyl iodide in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=20°C; 2 h;
2: With water-d2
Further stages.;
参考文献
Jin; Makioka; Kitamura; Fujiwara
Journal of Organic Chemistry, 2001 , vol. 66, # 2 p. 514 - 520
反应条件
hydrochloric ether; carbon dioxide in N,N-dimethyl-formamide
参考文献
Hess, U.; Thiele, R.
Journal fuer Praktische Chemie (Leipzig), 1982 , vol. 324, # 3 p. 385 - 399
反应条件
in benzene
6 h; Heating;
参考文献
Ismail, M. Fekry; El-Khamry, Abdel Momen A.; Abdel-Hamid, Hoda A.; Emara, Samir A.
Acta Chimica Hungarica, 1990 , vol. 127, # 1 p. 35 - 40
反应条件
piperidine in ethanol
6 h; Heating;
参考文献
Youssef, M. S. K.; Metwally, S. A. M.; El-Maghraby, M. A.; Younes, M. I.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 9 p. 878 - 881
反应条件
1.1: cyclopentyl-magnesium chloride / diethyl ether / 1.5 h / -30 °C / |Schlenk technique; |Inert atmosphere
2.1: 3 h / -30 °C / |Schlenk technique; |Inert atmosphere
3.1: air / methanol / -30 °C / |Schlenk technique; |Inert atmosphere
3.2: 0.5 h / |Schlenk technique; |Inert atmosphere
View Scheme
参考文献
Chen, Haoyi; Fan, Guoqin; Li, Shi; Mao, Kebin; Liu, Yuanhong
Tetrahedron Letters, 2014 , vol. 55, # 9 p. 1593 - 1596
反应条件
1: cyclopentyl-magnesium chloride / diethyl ether / 1.5 h / -30 °C / |Schlenk technique; |Inert atmosphere
2: 3 h / -30 °C / |Schlenk technique; |Inert atmosphere
3: hydrogenchloride; water / 0.5 h / 20 °C / |Schlenk technique; |Inert atmosphere
View Scheme
参考文献
Chen, Haoyi; Fan, Guoqin; Li, Shi; Mao, Kebin; Liu, Yuanhong
Tetrahedron Letters, 2014 , vol. 55, # 9 p. 1593 - 1596
反应条件
potassium tert-butylate in N,N-dimethyl-formamide
参考文献
Siegrist,A.E. et al.
Helvetica Chimica Acta, 1969 , vol. 52, p. 2521 - 2554
反应条件
potassium hydroxide in N,N-dimethyl-formamide
参考文献
Siegrist,A.E. et al.
Helvetica Chimica Acta, 1969 , vol. 52, p. 2521 - 2554
