2-(2-羟基苯基)六氟丙-2-醇合成路线 (共 3 条)
反应条件
AlCl3, aluminium chloride in 1,2-dichloro-ethane
T=-35 - 20°C; 36 h;
参考文献
LANXESS Deutschland GmbH
Patent: US2006/41149 A1, 2006 ;
Location in patent: Page/Page column 3 ;
反应条件
in 1,2,2-trifluoro-trichloroethane
T=80°C; 0.5 h;
参考文献
Dyachenko, V. I.; Kolomiets, A. F.; Fokin A. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, p. 2306 - 2310
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 11 p. 2557 - 2561
反应条件
in 1,2,2-trifluoro-trichloroethane
T=80°C; 0.5 h;
参考文献
Dyachenko, V. I.; Kolomiets, A. F.; Fokin A. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, p. 2306 - 2310
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 11 p. 2557 - 2561