1: Octa-1,7-diyne With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 0.5 h;
2: 2-(1,3-dioxolan-2-yl)ethyl iodide With N,N,N',N',N'',N''-hexamethylphosphoric triamide in tetrahydrofuran; hexane
T=-78 - 20°C; 16 h;
参考文献
Tokan, Wajdi M.; Meyer, Frank E.; Schweizer, Stefan; Parsons, Philip J.; De Meijere, Armin
European Journal of Organic Chemistry, 2008 , # 36 p. 6152 - 6167
