N-甲基-4-(二甲氨基)苄胺二盐酸盐合成路线 (共 3 条)
反应条件
1: in water; acetonitrile T=0°C; 2 h; Inert atmosphere; 2: With sodium cyanoborohydride in water; acetonitrile T=20°C; 4 h;
参考文献
UNIVERSITY OF CAPE TOWN; HUNTER, Roger; EGAN, Timothy John; ZISHIRI, Vincent Kudakwashe
Patent: WO2010/18555 A2, 2010 ;
Location in patent: Page/Page column 19; 29-30 ;
反应条件
sodium tetrahydroborate in methanol 11 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 53, # 20 p. 4667 - 4675
反应条件
sodium cyanoborohydride in methanol 72 h; Ambient temperature; Yield given;
参考文献
Archiv der Pharmazie (Weinheim, Germany), , vol. 320, # 7 p. 647 - 654