反应条件
1: 1) BuLi, 2) HMPA / 1) hexane, THF, -78 deg C, 20 min, 2) THF a) -78 deg C, 20 min, -40 deg C, 30 min 2: 92 percent / Bu4NF / tetrahydrofuran / 4 h / Ambient temperature 3: potassium carbonate, water / methanol / Ambient temperature View Scheme
参考文献
Cotterill, Ian C.; Jaouhari, Rabih; Dorman, Gyoergy; Roberts, Stanley M.; Scheinmann, Feodor; Wakefield, Basil J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 10 p. 2505 - 2512
