反应条件
in hexane
byproducts: Si2(CH3)6, C6H3(CH3)3, (CH3)3SiC6H2(CH3)3; Irradiation (UV/VIS); (Ar); photolysis of hexanes soln. of germanium compd. and dimethylbutadiene at -70°C for 24 h; evapn., chromy. (silica gel, hexanes) to isolate dimesitylgermacyclopentene deriv., thin layer chromy. (silica gel. hexanes), NMR and MAS;
参考文献
Hurni, Krysten L.; Baines, Kim M.
Canadian Journal of Chemistry, 2007 , vol. 85, # 10 p. 668 - 674