反应条件
1: 1.) aq. HCl, acetic acid, sodium nitrite, 2.) sodium acetate / 1.) 0 deg C, 2.) water, ethanol, RT, 3 h
2: 54 percent / sodium azide, hexadecyltributylphosphonium bromide / benzene; H2O / 24 h / 40 °C
3: 36 percent / diethyl ether / 4 h / Heating
4: 8 percent / 2-methoxy-ethanol / 20 h / Heating
View Scheme
参考文献
Bruche, Luca; Garanti, Luisa; Zecchi, Gaetano
Journal of Chemical Research, Miniprint, 1991 , # 1 p. 171 - 182
