2,4-二硝基-N,N-二乙基苯胺合成路线 （共 29 条）
反应条件
potassium carbonate in dimethyl sulfoxide
T=50°C; 3 h;
参考文献
Gale, Douglas J.; Rosevear, Judi; Wilshire, John F. K.
Australian Journal of Chemistry, 1995 , vol. 48, # 5 p. 997 - 1008
反应条件
in ethanol; water
T=60°C; 6 h;
参考文献
Bil'kis, I. I.; Uskov, S. I.; Galdikov, V. S.; Shteingarts, V. D.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 6 p. 1123 - 1130
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 6 p. 1247 - 1255
反应条件
1: 1.3 g / NaHCO3 / H2O; 2-methyl-propan-2-ol / 0 - 20 °C
2: 5.4 mg / diethyl ether / 1 h / -4 °C
View Scheme
参考文献
Saavedra; Srinivasan; Bonifant; Chu; Shanklin; Flippen-Anderson; Rice; Turpin; Davies; Keefer
Journal of Organic Chemistry, 2001 , vol. 66, # 9 p. 3090 - 3098
反应条件
T=100°C; P=6000480 Torr; 96 h;
参考文献
Matsumoto, Kiyoshi; Hashimoto, Shiro; Otani, Shinichi
Journal of the Chemical Society, Chemical Communications, 1991 , # 5 p. 306 - 307
反应条件
in diethyl ether
T=-4°C; 1 h;
参考文献
Saavedra; Srinivasan; Bonifant; Chu; Shanklin; Flippen-Anderson; Rice; Turpin; Davies; Keefer
Journal of Organic Chemistry, 2001 , vol. 66, # 9 p. 3090 - 3098
反应条件
in diethyl ether
T=-4°C; 1 h;
参考文献
Saavedra; Srinivasan; Bonifant; Chu; Shanklin; Flippen-Anderson; Rice; Turpin; Davies; Keefer
Journal of Organic Chemistry, 2001 , vol. 66, # 9 p. 3090 - 3098
参考文献
Brzozowski, Zdzisaw; Slawinski, Jarosaw
Synthetic Communications, 2010 , vol. 40, # 11 p. 1639 - 1645
参考文献
Chiriac, Constantin I.; Sava, Mitica; Tibirna, Mihaela; Chiriac, Florentina; Ropot, Radu; et al.
Revue Roumaine de Chimie, 1995 , vol. 40, # 11-12 p. 1197 - 1200
反应条件
sulfuric acid; nitric acid
man faellt mit Wasser;
参考文献
van Romburgh
Recueil des Travaux Chimiques des Pays-Bas, 1883 , vol. 2, p. 38
参考文献
Chiriac, Constantin I.; Sava, Mitica; Tibirna, Mihaela; Chiriac, Florentina; Ropot, Radu; et al.
Revue Roumaine de Chimie, 1995 , vol. 40, # 11-12 p. 1197 - 1200
