4,4-二苯基丁-3-烯-2-酮合成路线 （共 37 条）
反应条件
tert.-butylhydroperoxide; acetic anhydride; p-benozquinone; palladium diacetate in acetic acid
12 h; Heating;
参考文献
Jia, Chengguo; Lu, Wenjun; Kitamura, Tsugio; Fujiwara, Yuzo
Organic Letters, 1999 , vol. 1, # 13 p. 2097 - 2100
反应条件
sodium acetate; propionic acid; palladium diacetate in benzene
参考文献
Ishii, Yasutaka; Nakano, Tatsuya
Patent: US2003/171625 A1, 2003 ;
反应条件
formic acid; triethylamine; [Pd(PPh3)2(OAc)2] in acetonitrile
T=80°C; 12 h;
参考文献
Cacchi, S.; Palmieri, G.
Synthesis, 1984 , # 7 p. 575 - 577
反应条件
potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)); Tedicyp in N,N-dimethyl-formamide
T=130°C; Heck reaction; 20 h;
参考文献
Kondolff, Isabelle; Doucet, Henri; Santelli, Maurice
Tetrahedron Letters, 2003 , vol. 44, # 46 p. 8487 - 8491
反应条件
oxygen; caesium acetate; palladium dichloride in N,N-dimethyl acetamide; acetonitrile
T=20 - 80°C; 16.1667 h; Large scale reaction;
参考文献
Rosa, David; Orellana, Arturo
Organic Letters, 2011 , vol. 13, # 14 p. 3648 - 3651
反应条件
tetrabutyl-ammonium chloride; sodium acetate; palladium diacetate in N,N-dimethyl-formamide
T=60°C; 8 h;
参考文献
Amorese, A.; Arcadi, A.; Bernocchi, E.; Cacchi, S.; Cerrini, S.; et al.
Tetrahedron, 1989 , vol. 45, # 3 p. 813 - 828
反应条件
potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)); Tedicyp in N,N-dimethyl-formamide
T=130°C; Heck reaction; 20 h;
参考文献
Kondolff, Isabelle; Doucet, Henri; Santelli, Maurice
Tetrahedron Letters, 2003 , vol. 44, # 46 p. 8487 - 8491
反应条件
α-cyclohexylcyclohexanemethanamine; 1-(4-hydroxyphenyl)ethanone oxime in water
Heck reaction; 8 h; Heating;
参考文献
Botella, Luis; Najera, Carmen
Tetrahedron Letters, 2004 , vol. 45, # 9 p. 1833 - 1836
反应条件
chloroform; palladium diacetate; caesium carbonate; triphenylphosphine in toluene
T=80°C; 24 h; Inert atmosphere;
参考文献
Yamamoto, Tetsuya; Iizuka, Michiko; Takenaka, Hiroto; Ohta, Tetsuo; Ito, Yoshihiko
Journal of Organometallic Chemistry, 2009 , vol. 694, # 9-10 p. 1325 - 1332
反应条件
tetrakis(triphenylphosphine) palladium(0); copper(I) thiophene-2-carboxylate; potassium carbonate; 1,2-bis-(diphenylphosphino)ethane in tetrahydrofuran
T=50°C; Liebeskind-Srogl cross-coupling; 13 h; Inert atmosphere;
参考文献
Jin, Weiwei; Du, Wangming; Yang, Qin; Yu, Haifeng; Chen, Jiping; Yu, Zhengkun
Organic Letters, 2011 , vol. 13, # 16 p. 4272 - 4275
