反应条件
1: 82 percent / 1.) n-BuLi, 2.) HMPTA / 1.) benzene-THF, 20 deg C, 2 h, 2.) 20 deg C, 12 h
2: 98 percent / H2 / Lindlar catalyst / quinoline / 15 °C
3: 2.4 g / 1.) i-Bu2LiH, 2.) air, 3.) O2 / 1.) toluene, reflux, 7 h, 2.) 20 deg C, 3.) 60 - 65 deg C, 3 h; other reagent
4: 97 percent / pyridine / 3 h / 50 °C
View Scheme
参考文献
Zakharkin, L. I.; Petrushkina, E. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, p. 1683 - 1684
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 8 p. 1892 - 1893
