2-(二甲基氨基)-8-苯基-4H-1-苯并吡喃-4-酮合成路线 （共 2 条）
反应条件
1: N,N,N',N'-Tetramethylmalonsaeurediamid With trichlorophosphate
T=20°C; 0.5 h;
2: 2-hydroxybiphenyl in chlorobenzene
T=100°C; 4 h;
3: With sodium acetate in water; chlorobenzene
T=80°C; 1.5 h;
参考文献
Sottofattori, Enzo; Anzaldi, Maria; Mazzei, Mauro; Miele, Mariangela; Balbi, Alessandro; Pyshnyi, Dmitri S.; Zakharova, Olga D.; Abramova, Tatyana V.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 5 p. 1515 - 1522
反应条件
1: phosphylchloride / 0.5 h / Ambient temperature
2: chlorobenzene / 5 h / Heating
3: 3.99 g / CH3COONa*3H2O / chlorobenzene; H2O / 1.5 h / 90 - 95 °C
View Scheme
参考文献
Balbi; Roma; Ermili; Ambrosini; Passerini
Farmaco, Edizione Scientifica, 1982 , vol. 37, # 9 p. 582 - 596
