5-(三氟甲基)-2-嘧啶酮合成路线 （共 5 条）
反应条件
hydrogenchloride
T=50°C; 0.666667 h;
参考文献
Benneche, Tore; Undheim, Kjell
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1984 , vol. 38, # 6 p. 505 - 508
反应条件
sodium hydroxide
0.166667 h; Ambient temperature;
参考文献
Benneche, Tore; Undheim, Kjell
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1984 , vol. 38, # 6 p. 505 - 508
反应条件
1: 1.) HCl, 2.) N-chlorosuccinimide / 2.) CCl4, irradiation, reflux, 4 h
2: 51 percent / SbF5 / 1.) 50 deg C, 35 min, 2.) 150 deg C, 15 min
3: 83 percent / aq. HCl / 0.67 h / 50 °C
View Scheme
参考文献
Benneche, Tore; Undheim, Kjell
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1984 , vol. 38, # 6 p. 505 - 508
反应条件
1: 51 percent / SbF5 / 1.) 50 deg C, 35 min, 2.) 150 deg C, 15 min
2: 83 percent / aq. HCl / 0.67 h / 50 °C
View Scheme
参考文献
Benneche, Tore; Undheim, Kjell
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1984 , vol. 38, # 6 p. 505 - 508
反应条件
1: 76 percent / m-chloroperbenzoic acid / CH2Cl2 / 24 h / Ambient temperature
2: 67 percent / 1 M NaOH / 0.17 h / Ambient temperature
View Scheme
参考文献
Benneche, Tore; Undheim, Kjell
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1984 , vol. 38, # 6 p. 505 - 508
