三甲基[2-[(三甲基硅烷基)甲基]苄基]碘化铵合成路线 (共 5 条)
反应条件
tetrabutyl ammonium fluoride in acetonitrile Ambient temperature;
参考文献
Trahanovsky, Walter S.; Marcias, James R.
Journal of the American Chemical Society, 1986 , vol. 108, # 21 p. 6820 - 6821
反应条件
1: 1.) n-BuLi, 2.) Et3N / 1.) Et2O, room temperatutre, 22 h, 2.) room temperature, 4 h
2: acetonitrile / 1 h / Heating
View Scheme
参考文献
Ito; Nakatsuka; Saegusa
Journal of the American Chemical Society, 1982 , vol. 104, # 26 p. 7609 - 7622
反应条件
in acetonitrile
1 h; Heating; Yield given;
参考文献
Ito; Nakatsuka; Saegusa
Journal of the American Chemical Society, 1982 , vol. 104, # 26 p. 7609 - 7622
反应条件
tetrabutyl ammonium fluoride in acetonitrile-D3
flow rate: 45 mL/min;
参考文献
Trahanovsky, Walter S.; Chou, C. -H.; Fischer, D. R.; Gerstein, B. C.
Journal of the American Chemical Society, 1988 , vol. 110, # 19 p. 6579 - 6581
反应条件
fluoride in acetonitrile
Elimination; Diels-Alder reaction;
参考文献
Di Valentin, Cristiana; Freccero, Mauro; Sarzi-Amade, Mirko; Zanaletti, Riccardo
Tetrahedron, 2000 , vol. 56, # 16 p. 2547 - 2559