5-甲氧基-四氢萘-2-甲酸甲酯合成路线 (共 7 条)
反应条件
palladium in methanol
参考文献
Fujisawa Pharmaceutical Co., Ltd.
Patent: US5763489 A1, 1998 ;
反应条件
1: 80 percent / N-nromosuccinimide, benzoyl peroxide / CCl4 / 12 h / Heating
2: 85 percent / ethanol; H2O / 0.25 h / Ambient temperature
3: 80 percent / benzene; diethyl ether / 36 h / Ambient temperature
4: 97 percent
5: CsF / acetonitrile / 1 h / Ambient temperature
View Scheme
参考文献
Ito; Nakatsuka; Saegusa
Journal of the American Chemical Society, 1982 , vol. 104, # 26 p. 7609 - 7622
反应条件
1: 85 percent / ethanol; H2O / 0.25 h / Ambient temperature
2: 80 percent / benzene; diethyl ether / 36 h / Ambient temperature
3: 97 percent
4: CsF / acetonitrile / 1 h / Ambient temperature
View Scheme
参考文献
Ito; Nakatsuka; Saegusa
Journal of the American Chemical Society, 1982 , vol. 104, # 26 p. 7609 - 7622
反应条件
1: 80 percent / benzene; diethyl ether / 36 h / Ambient temperature
2: 97 percent
3: CsF / acetonitrile / 1 h / Ambient temperature
View Scheme
参考文献
Ito; Nakatsuka; Saegusa
Journal of the American Chemical Society, 1982 , vol. 104, # 26 p. 7609 - 7622
反应条件
1: 97 percent
2: CsF / acetonitrile / 1 h / Ambient temperature
View Scheme
参考文献
Ito; Nakatsuka; Saegusa
Journal of the American Chemical Society, 1982 , vol. 104, # 26 p. 7609 - 7622
反应条件
cesium fluoride in acetonitrile
1 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Ito; Nakatsuka; Saegusa
Journal of the American Chemical Society, 1982 , vol. 104, # 26 p. 7609 - 7622
反应条件
ammonium nitrate in methanol
T=25°C; Electrochemical reaction; Title compound not separated from byproducts;
参考文献
Kise, Naoki; Mimura, Ryosuke; Ueda, Nasuo
Bulletin of the Chemical Society of Japan, 2002 , vol. 75, # 12 p. 2693 - 2694