反应条件
1: 1.)NaH, 2.) tosyl azide
2: potassium hydroxide / methanol / 3 h / Heating
3: 68 percent / pyridine / benzene / 1 h / 80 °C
4: 90 percent / acetic acid / 5 h / Ambient temperature
5: lithium aluminium hydride / diethyl ether / 1 h / Ambient temperature
View Scheme
参考文献
Sakai, Yasuo; Toyotani, Shingo; Ohtani, Masaru; Matsumoto, Masaharu; Tobe, Yoshito; Odaira, Yoshinobu
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 5 p. 1474 - 1480
