反应条件
1.1: AlCl3, aluminium chloride / dichloromethane / -10 °C 1.2: 10 h / 5 - 20 °C 2.1: potassium hydrogencarbonate / anhydrous xylene; water / 12 h / Reflux 3.1: sodium tetrahydroborate / methanol / 0.5 h / Cooling with ice 4.1: 1H-imidazole / N,N-dimethyl-formamide / 10.25 h / 0 - 20 °C / Inert atmosphere 5.1: N-bromosuccinmide; dihydrogen peroxide / tetrachloromethane / 4 h / Reflux 6.1: magnesium / tetrahydrofuran / 2 h / Inert atmosphere 6.2: 4 h / Inert atmosphere 6.3: 4 h / Inert atmosphere 7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / Inert atmosphere View Scheme
参考文献
Synthetic Communications, , vol. 41, # 15 p. 2296 - 2303
