4-甲氧基-4'-甲基二苯甲醇合成路线 （共 37 条）
反应条件
1: Na, EtOH View Scheme
参考文献
Errede,L.A. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 5224 - 5227
反应条件
potassium 12-tungstocobalt(III)ate; sodium tartrate buffer in water pH=4.0; 48 h;
参考文献
Bietti, Massimo; Lanzalunga, Osvaldo
Journal of Organic Chemistry, 2002 , vol. 67, # 8 p. 2632 - 2638
反应条件
1: iodine / dichloromethane / 1 h / 25 °C 2: iodine / neat (no solvent) / 4 h / 85 °C View Scheme
参考文献
Jereb, Marjan; Vrazic, Dejan
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 12 p. 1978 - 1999
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; [rhodium(I)(carbonyl)2(acetylacetonate)] in 1,4-dioxane
T=95°C; 16 h;
参考文献
Sakai, Masaaki; Ueda, Masato; Miyaura, Norio
Angewandte Chemie - International Edition, 1998 , vol. 37, # 23 p. 3279 - 3281
反应条件
C42H62ClO3PPd; sodium salt of phosphorous acid in toluene
T=50°C; 36 h;
参考文献
Liao, Yuan-Xi; Xing, Chun-Hui; Israel, Matthew; Hu, Qiao-Sheng
Tetrahedron Letters, 2011 , vol. 52, # 26 p. 3324 - 3328
反应条件
octyne-4; water; bis(1,5-cyclooctadiene)nickel (0) in 1,4-dioxane
T=80°C; 12 h;
参考文献
Takahashi, Go; Shirakawa, Eiji; Tsuchimoto, Teruhisa; Kawakami, Yusuke
Chemical Communications, 2005 , # 11 p. 1459 - 1461
反应条件
Ni(Br)2(dppe); zinc in tetrahydrofuran
T=75°C; Arylation; 24 h;
参考文献
Majumdar, Kanak Kanti; Cheng, Chien-Hong
Organic Letters, 2000 , vol. 2, # 15 p. 2295 - 2297
反应条件
Cp2Fe in THF-d8 (tetrahydrofuran-d8); water-d2
under N2, standard Schlenk techniques; in NMR tube; THF-d8 added to mixt. of Rh complex and Cp2Fe (small amt.); aldehyde (20 equiv.) added; degassed D2O added; stirred at room temp. for 40 h; not isolated; monitored by (1)H NMR spectra;
参考文献
Krug, Christopher; Hartwig, John F.
Journal of the American Chemical Society, 2002 , vol. 124, # 8 p. 1674 - 1679
反应条件
potassium phosphate; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in tetrahydrofuran; water
T=20°C; 16 h;
参考文献
Xing, Chun-Hui; Liu, Tao-Ping; Zheng, Jin Rong; Ng, Jaclynn; Esposito, Michelle; Hu, Qiao-Sheng
Tetrahedron Letters, 2009 , vol. 50, # 35 p. 4953 - 4957
反应条件
potassium phosphate; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in tetrahydrofuran; water
T=20°C; 19 h;
参考文献
Xing, Chun-Hui; Liu, Tao-Ping; Zheng, Jin Rong; Ng, Jaclynn; Esposito, Michelle; Hu, Qiao-Sheng
Tetrahedron Letters, 2009 , vol. 50, # 35 p. 4953 - 4957
