4-甲氧基-4'-甲基二苯甲醇合成路线 (共 37 条)
反应条件
1: para-bromotoluene With magnesium in diethyl ether
2: 4-methoxy-benzaldehyde in diethyl ether
Grignard reaction; Further stages.;
参考文献
Denegri, Bernard; Kronja, Olga
Journal of Organic Chemistry, 2007 , vol. 72, # 22 p. 8427 - 8433
反应条件
hydrogenchloride; sodium in toluene
参考文献
K I CHEMICAL INDUSTRY CO., LTD.
Patent: EP801048 A1, 1997 ;
反应条件
1: With [2,2']bipyridinyl; sodium acetate; copper(l) chloride in o-xylene
T=135°C; 6 h;
2: With hydrogenchloride in o-xylene; water
参考文献
Liao, Yuan-Xi; Hu, Qiao-Sheng
Journal of Organic Chemistry, 2011 , vol. 76, # 18 p. 7602 - 7607
反应条件
1: tetrahydrofuran
2: Cp2Fe / THF-d8 (tetrahydrofuran-d8); water-d2
View Scheme
参考文献
Krug, Christopher; Hartwig, John F.
Journal of the American Chemical Society, 2002 , vol. 124, # 8 p. 1674 - 1679
反应条件
in tetrahydrofuran
T=0 - 20°C; 1 h;
参考文献
Krug, Christopher; Hartwig, John F.
Journal of the American Chemical Society, 2002 , vol. 124, # 8 p. 1674 - 1679
反应条件
water in acetonitrile
T=20°C; Flash photolysis; Kinetics;
参考文献
Minegishi, Shinya; Kobayashi, Shinjiro; Mayr, Herbert
Journal of the American Chemical Society, 2004 , vol. 126, # 16 p. 5174 - 5181
反应条件
water in acetonitrile
T=20°C; Flash photolysis; Kinetics; Further Variations:water/acetonitrile ratio dependence;
参考文献
Minegishi, Shinya; Kobayashi, Shinjiro; Mayr, Herbert
Journal of the American Chemical Society, 2004 , vol. 126, # 16 p. 5174 - 5181
反应条件
2,6-dimethylpyridine; water in acetone
T=25°C; Kinetics; Further Variations:SolventsReagents;
参考文献
Denegri, Bernard; Minegishi, Shinya; Kronja, Olga; Mayr, Herbert
Angewandte Chemie - International Edition, 2004 , vol. 43, # 17 p. 2302 - 2305
反应条件
sodium tetrahydroborate in isopropyl alcohol
参考文献
Mindl,J.; Vecera,M.
Collection of Czechoslovak Chemical Communications, 1972 , vol. 37, p. 1143 - 1149
反应条件
water in sulfuric acid; acetic acid
Equilibrium constant;
参考文献
Mindl,J.
Collection of Czechoslovak Chemical Communications, 1972 , vol. 37, p. 585 - 591