2,5-二苯基-1H-吡咯合成路线 （共 63 条）
反应条件
potassium hydroxide in dimethyl sulfoxide
T=45°C; 8 h;
参考文献
Yurovskaya, M. A.; Afanas'ev, A. Z.; Bundel', Yu. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1984 , vol. 20, # 8 p. 875 - 877
Khimiya Geterotsiklicheskikh Soedinenii, 1984 , vol. 20, # 8 p. 1077 - 1079
反应条件
titanium tetrachloride; triethylamine in dichloromethane
T=0 - 25°C; 10 h;
参考文献
Periasamy, Mariappan; Srinivas, Gadthula; Seenivasaperumal, Muthu
Journal of Chemical Research, 2004 , # 4 p. 270 - 272
反应条件
1: acetophenone oxime With sodium hydroxide in dimethyl sulfoxide
T=100 - 105°C; 2 h;
2: phenylacetylene in dimethyl sulfoxide
T=140°C; 4 h;
参考文献
Petrova; Mikhaleva; Sobenina; Trofimov
Russian Journal of Organic Chemistry, 2010 , vol. 46, # 3 p. 452 - 454
反应条件
sodium hydrogensulfite; copper(I) bromide in dimethyl sulfoxide
T=140°C; 2 h; Inert atmosphere;
参考文献
Ran, Longfei; Ren, Zhi-Hui; Wang, Yao-Yu; Guan, Zheng-Hui
Green Chemistry, 2014 , vol. 16, # 1 p. 112 - 115
反应条件
sodium hydroxide in ethanol; water
Heating; Yield given;
参考文献
Itahara, Toshio
Journal of the Chemical Society, Chemical Communications, 1981 , # 5 p. 254 - 255
反应条件
1: triethylamine / CH2Cl2 / 0.75 h / 20 °C
2: 90 percent / NaN3 / dimethylformamide / 17.5 h / 20 °C
3: 82 percent / PtCl4; 2,6-di-tert-butyl-4-methylpyridine / 1,2-dichloro-ethane / 0.83 h / Heating
View Scheme
参考文献
Hiroya, Kou; Matsumoto, Shigemitsu; Ashikawa, Masayasu; Ogiwara, Kentaro; Sakamoto, Takao
Organic Letters, 2006 , vol. 8, # 23 p. 5349 - 5352
反应条件
in toluene
6 h; UV-irradiationInert atmosphere;
参考文献
Muthukrishnan, Sivaramakrishnan; Sankaranarayanan, Jagadis; Klima, Rodney F.; Pace, Tamara C. S.; Bohne, Cornelia; Gudmundsdottir, Anna D.
Organic Letters, 2009 , vol. 11, # 11 p. 2345 - 2348
反应条件
lithium hydroxide in dimethyl sulfoxide
T=130°C; 5 h;
参考文献
Shmidt; Zorina; Mikhaleva; Ushakov; Skital'Tseva; Trofimov
Russian Journal of Organic Chemistry, 2010 , vol. 46, # 3 p. 457 - 458
反应条件
potassium hydroxide; Propylene glycol
参考文献
Henze; Shown
Journal of the American Chemical Society, 1947 , vol. 69, p. 1662,1665
反应条件
sodium hydroxide in ethanol; water
T=70°C; 7 h; Yield given;
参考文献
Itahara, Toshio
Journal of the Chemical Society, Chemical Communications, 1981 , # 5 p. 254 - 255
