Lee, Jeewoo; Lee, Ju-Hyun; Kim, Su Yeon; Perry, Nicholas A.; Lewin, Nancy E.; Ayres, Jolene A.; Blumberg, Peter M.
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 6 p. 2022 - 2031
Lee, Jeewoo; Lee, Ju-Hyun; Kim, Su Yeon; Perry, Nicholas A.; Lewin, Nancy E.; Ayres, Jolene A.; Blumberg, Peter M.
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 6 p. 2022 - 2031
1: potassium hydroxide, water / ethane-1,2-diol / 18 h / Heating 2: oxalyl chloride, DMF / benzene / 1 h / 20 °C 3: sodium hydrogen carbonate / CH2Cl2; H2O / 1.5 h 4: phosphorus oxychloride / acetonitrile / 0.42 h / Heating 5: sodium borohydride / methanol / 0.75 h / 0 °C 6: hydrogen, conc. hydrochloric acid / 10percent palladium-charcoal / ethanol / 2 h View Scheme
参考文献
Battersby, Alan R.; Jones, Raymond C. F.; Kazlauskas, Rymantas; Thornber, Craig W.; Ruchirawat, Somsak; Staunton, James
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2016 - 2029
