2,4,5-三甲氧基苯甲酸酐合成路线 (共 2 条)
反应条件
potassium hydroxide; potassium asaronate 1.) 180 deg C, 15 Torr, 4 h, 2.) aq. ethanol, reflux, 0.5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Patwardhan, Sarita A.; Gupta, Amrit S.
Journal of Chemical Research, Miniprint, 1984 , # 12 p. 3786 - 3795
反应条件
methanesulfonyl chloride; triethylamine in tetrahydrofuran
T=0°C;
参考文献
Daskiewicz, Jean-Baptiste; Depeint, Flore; Viornery, Lionel; Bayet, Christine; Comte-Sarrazin, Geraldine; Comte, Gilles; Gee, Jennifer M.; Johnson, Ian T.; Ndjoko, Karine; Hostettmann, Kurt; Barron, Denis
Journal of Medicinal Chemistry, 2005 , vol. 48, # 8 p. 2790 - 2804