1: 94 percent / MeSO3H / 17 h / 0 - 20 °C
2: 92 percent / Et3N / CCl4 / 17 h / 0 - 20 °C
3: 63 percent / liquid NH3; Li / tetrahydrofuran / 2 h / -78 °C
View Scheme
参考文献
Huffman, John W.; Miller, John R. A.; Liddle, John; Yu, Shu; Thomas, Brian F.; Wiley, Jenny L.; Martin, Billy R.
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 7 p. 1397 - 1410
1: 94 percent / MeSO3H / 17 h / 0 - 20 °C
2: 92 percent / Et3N / CCl4 / 17 h / 0 - 20 °C
3: 63 percent / liquid NH3; Li / tetrahydrofuran / 2 h / -78 °C
View Scheme
参考文献
Huffman, John W.; Miller, John R. A.; Liddle, John; Yu, Shu; Thomas, Brian F.; Wiley, Jenny L.; Martin, Billy R.
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 7 p. 1397 - 1410
1: 92 percent / Et3N / CCl4 / 17 h / 0 - 20 °C
2: 63 percent / liquid NH3; Li / tetrahydrofuran / 2 h / -78 °C
View Scheme
参考文献
Huffman, John W.; Miller, John R. A.; Liddle, John; Yu, Shu; Thomas, Brian F.; Wiley, Jenny L.; Martin, Billy R.
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 7 p. 1397 - 1410
