3,7-二溴二苯并[b,d]噻吩合成路线 （共 5 条）
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Eisch, John J.; Hallenbeck, Lawrence E.; Han, Kyoung Im
Journal of the American Chemical Society, 1986 , vol. 108, # 24 p. 7763 - 7767
反应条件
1: 55 percent / bromine
3: 71 percent / LiAlH4 / diethyl ether
View Scheme
参考文献
Eisch, John J.; Hallenbeck, Lawrence E.; Han, Kyoung Im
Journal of the American Chemical Society, 1986 , vol. 108, # 24 p. 7763 - 7767
反应条件
2: 71 percent / LiAlH4 / diethyl ether
View Scheme
参考文献
Eisch, John J.; Hallenbeck, Lawrence E.; Han, Kyoung Im
Journal of the American Chemical Society, 1986 , vol. 108, # 24 p. 7763 - 7767
反应条件
1: 15 percent / lithium aluminium hydride, (2,2'-bipyridyl)(1,5-cyclooctadiene)nickel / tetrahydrofuran / 48 h / 55 °C
2: 55 percent / bromine
4: 71 percent / LiAlH4 / diethyl ether
View Scheme
参考文献
Eisch, John J.; Hallenbeck, Lawrence E.; Han, Kyoung Im
Journal of the American Chemical Society, 1986 , vol. 108, # 24 p. 7763 - 7767
反应条件
FeCl3 in 1-methyl-pyrrolidin-2-one; hydrogenchloride
参考文献
The University of North Carolina at Chapel Hill
Patent: US6172104 B2, 2001 ;
