4-(6-羟基己氧基)苯甲酸合成路线 （共 18 条）
反应条件
1: K2CO3 / butan-2-one
2: aq. KOH / ethanol
View Scheme
参考文献
Aldred, Matthew P.; Vlachos, Panos; Contoret, Adam E. A.; Farrar, Simon R.; Chung-Tsoi; Mansoor, Bassam; Woon, Kai L.; Hudson, Robert; Kelly, Stephen M.; O'Neill, Mary
Journal of Materials Chemistry, 2005 , vol. 15, # 31 p. 3208 - 3213
反应条件
1: water / ethanol
2: potassium hydroxide; potassium iodide
View Scheme
参考文献
Hu, Jian-She; Li, Dan; Zhang, Wen-Chang; Meng, Qing-Bao
Journal of Polymer Science, Part A: Polymer Chemistry, 2012 , vol. 50, # 24 p. 5049 - 5059
反应条件
1: sodium hydroxide; potassium iodide / acetone / 20 h / 60 °C
2: potassium hydroxide / water / 6 h / 60 °C
View Scheme
参考文献
Chen, Xingwu; Wang, Ling; Chen, Yinjie; Li, Chenyue; Hou, Guoyan; Liu, Xin; Zhang, Xiaoguang; He, Wanli; Yang, Huai
Chemical Communications, 2014 , vol. 50, # 6 p. 691 - 694
反应条件
1: sulfuric acid / 12 h / Reflux
2: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 48 h / 90 °C
3: potassium hydroxide / methanol / 12 h / 50 °C
View Scheme
参考文献
Ramkumar; Amala Rose; Ramakrishnan
Journal of Polymer Science, Part A: Polymer Chemistry, 2010 , vol. 48, # 14 p. 3200 - 3209
反应条件
1: 6-hydroxy-1-hexanol With potassium iodide; potassium hydroxide
2: 4-hydroxy-benzoic acid
参考文献
Hu, Jian-She; Li, Dan; Zhang, Wen-Chang; Meng, Qing-Bao
Journal of Polymer Science, Part A: Polymer Chemistry, 2012 , vol. 50, # 24 p. 5049 - 5059
反应条件
1: 67 percent / hydroquinone, p-toluenesulphonic acid / benzene / 20 h / Heating
2: 1.) thionyl chloride, 2,6-di-tert-butyl-4-methyl phenol, DMF; 2.) triethylamine / 1.) 25 min; 2.) chloroform, room t., 24 h
View Scheme
参考文献
Cowie, J. M. G.; Hunter, H. W.
Canadian Journal of Chemistry, 1995 , vol. 73, p. 1811 - 1817
参考文献
Palani; Saravanan; Kannan
Journal of Chemical Sciences, 2011 , vol. 123, # 1 p. 81 - 89
反应条件
toluene-4-sulfonic acid; hydroquinone in chloroform
12 h;
参考文献
Contoret, Adam; Farrar, Simon; Jackson, Perregrin; Kelly, Stephen M.; Khan, Sultan; Nicholls, Edward; Oneill, Mary; Richards, Gary
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2001 , vol. 364, p. 511 - 518
