1,3,5-三(2-羟乙基)氰尿酸合成路线 （共 3 条）
反应条件
sodium hydride 1.) HMPA, 100 deg C, 3 h, 2.) HMPA, 100 deg C, 7 h; Yield given. Multistep reaction;
参考文献
Synthetic Communications, , vol. 23, # 19 p. 2659 - 2672
反应条件
1: 100 percent / SOCl2 / dioxane 2: 2) H2 / 2) 5percent Pd on C / 2) MeOH, HOAc View Scheme
参考文献
Askew, Benny C.
Tetrahedron Letters, 1990 , vol. 31, # 30 p. 4245 - 4248
反应条件
1: 1,3,5-tris(2-hydroxyethyl)-S-triazine-2,4,6(1H,3H,5H)-trione With sodium hydride in dimethyl sulfoxide
T=20°C; Inert atmosphereCooling with ice;
2: propargyl bromide in dimethyl sulfoxide; toluene
T=35 - 40°C; Inert atmosphere;
参考文献
Piron, Flavia; Oprea, Cornelia; Cisma, Crinas; Terec, Anamaria; Roncali, Jean; Grosu, Ion
Synthesis, 2010 , # 10 art. no. P01810SS, p. 1639 - 1644
