N-(3-溴苯基)甲烷磺酰胺合成路线 （共 4 条）
反应条件
pyridine in dichloromethane T=10 - 20°C; 15 h;
参考文献
AURIGENE DISCOVERY TECHNOLOGIES LIMITED; UM PHARMAUJI SDN. BHD; GUMMADI, Venkateshwar, Rao; HOSAHALLI, Subramanya; NANDURI, Srinivas; AGGUNDA RENUKAPPA, Girish
Patent: WO2014/6554 A1, 2014 ;
Location in patent: Page/Page column 28 ;
反应条件
1.1: Et3N / methanol 2.1: TfOH / CH2Cl2 / 0.17 h / 20 °C 2.2: KOH / dimethylsulfoxide / 80 °C View Scheme
参考文献
Tokuyama, Hidetoshi; Sato, Masashi; Ueda, Toshihiro; Fukuyama, Tohru
Heterocycles, 2001 , vol. 54, # 1 p. 105 - 108
反应条件
1.1: Et3N / methanol 2.1: TfOH / CH2Cl2 / 0.17 h / 20 °C 2.2: KOH / dimethylsulfoxide / 80 °C View Scheme
参考文献
Tokuyama, Hidetoshi; Sato, Masashi; Ueda, Toshihiro; Fukuyama, Tohru
Heterocycles, 2001 , vol. 54, # 1 p. 105 - 108
反应条件
1: in ethylene glycol dimethyl ether 0.166667 h; Inert atmosphere; 2: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate in ethylene glycol dimethyl ether T=80°C; Inert atmosphere;
参考文献
AURIGENE DISCOVERY TECHNOLOGIES LIMITED; UM PHARMAUJI SDN. BHD; GUMMADI, Venkateshwar, Rao; HOSAHALLI, Subramanya; NANDURI, Srinivas; AGGUNDA RENUKAPPA, Girish
Patent: WO2014/6554 A1, 2014 ;
Location in patent: Page/Page column 28 ;
