二甲基甲氧基苯并二氢吡喃醇合成路线 （共 4 条）
反应条件
lithium aluminium tetrahydride in diethyl ether
0.5 h; Heating;
参考文献
Anastasis, Panayiotis; Brown, Philip E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 9 p. 2013 - 2018
反应条件
1: 48 percent / polyphosphoric acid / 1.) 30 deg C, 4 h, 100 deg C, 1 h
2: 87 percent / LiAlH4 / diethyl ether / 0.5 h / Heating
View Scheme
参考文献
Anastasis, Panayiotis; Brown, Philip E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 9 p. 2013 - 2018
反应条件
1: 48 percent / polyphosphoric acid / 1.) 30 deg C, 4 h, 100 deg C, 1 h
2: 87 percent / LiAlH4 / diethyl ether / 0.5 h / Heating
View Scheme
参考文献
Anastasis, Panayiotis; Brown, Philip E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 9 p. 2013 - 2018
反应条件
hydrogenchloride; zinc
Reduction; cyclization; 0.0833333 h;
参考文献
Yenes, Susana; Messeguer, Angel
Tetrahedron, 1999 , vol. 55, # 49 p. 14111 - 14122
