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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
83925-76-2
合成路线
(共 7 条)
344417-07-8
+
124-63-0
甲烷磺酰氯
→
反应条件
51599-68-9
1-(甲基磺酰基)吡咯烷
+
83925-76-2
+
89717-39-5
反应条件
triethylamine in benzene 24 h; Ambient temperature;
参考文献
Fatutta, Silvana; Pitacco, Giuliana; Valentin, Ennio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 11 p. 2735 - 2738
83925-72-8
→
反应条件
83925-76-2
反应条件
1: 87 percent / 24 h / Heating 2: H2O View Scheme
参考文献
Fatutta, Silvana; Pitacco, Giuliana; Russo, Claudio; Valentin, Ennio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 9 p. 2045 - 2050
344417-07-8
→
反应条件
83925-76-2
+
89717-35-1
反应条件
water; methyl iodide 1.) acetonitrile, reflux, 12 h, 2.) RT; Multistep reaction. Yields of byproduct given;
参考文献
Fatutta, Silvana; Pitacco, Giuliana; Valentin, Ennio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 11 p. 2735 - 2738
344417-07-8
+
75-36-5
乙酰氯
→
反应条件
83925-76-2
+
89717-36-2
反应条件
water 1.) benzene, reflux, 3 h, 2.) RT, ethanol, 24 h; Yield given. Multistep reaction;
参考文献
Fatutta, Silvana; Pitacco, Giuliana; Valentin, Ennio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 11 p. 2735 - 2738
344417-07-8
+
74-88-4
甲基碘
→
反应条件
83925-76-2
+
89717-35-1
反应条件
water 1.) acetonitrile, reflux, 12 h, 2.) RT; Yield given. Multistep reaction;
参考文献
Fatutta, Silvana; Pitacco, Giuliana; Valentin, Ennio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 11 p. 2735 - 2738
98-88-4
苯甲酰氯
+
344417-07-8
→
反应条件
83925-76-2
+
3389-54-6
苯基(1-吡咯烷基)甲酮
+
89717-37-3
+
89717-38-4
反应条件
water 1.) benzene, reflux, 24 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Fatutta, Silvana; Pitacco, Giuliana; Valentin, Ennio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 11 p. 2735 - 2738
110-91-8
吗啉
+
83925-76-2
→
反应条件
89717-29-3
反应条件
in benzene
参考文献
Fatutta, Silvana; Pitacco, Giuliana; Valentin, Ennio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 11 p. 2735 - 2738