反式-2-苯乙烯硼酸频哪酸酯合成路线 （共 45 条）
反应条件
methanol; bis[2-(diphenylphosphino)phenyl] ether; sodium t-butanolate; copper(l) chloride in tetrahydrofuran T=20°C; 24 h;
参考文献
Jung, Ho-Young; Feng, Xinhui; Kim, Hyohyun; Yun, Jaesook
Tetrahedron, 2012 , vol. 68, # 17 p. 3444 - 3449
反应条件
in tetrahydrofuran T=23°C; 3 h;
参考文献
Yoo, Kyung Soo; Yoon, Cheol Hwan; Jung, Kyung Woon
Journal of the American Chemical Society, 2006 , vol. 128, # 50 p. 16384 - 16393
反应条件
bis(cyclohexanyl)borane T=20°C; 2 h;
参考文献
Shirakawa, Kazuya; Arase, Akira; Hoshi, Masayuki
Synthesis, 2004 , # 11 p. 1814 - 1820
反应条件
in tetrahydrofuran T=20°C; 18 h;
参考文献
Synthesis, , # 11 p. 1814 - 1820
反应条件
triethylamine; dichloro bis(acetonitrile) palladium(II) in 1,4-dioxane T=110°C; 4 h;
参考文献
Billingsley, Kelvin L.; Buchwald, Stephen L.
Journal of Organic Chemistry, 2008 , vol. 73, # 14 p. 5589 - 5591
反应条件
(CH3Si(C6H4P(C6H3(CF3)2)2)2)Pd(SO3CF3); triethylaluminum in toluene T=20°C; 24 h; Inert atmosphere; diastereoselective reaction;
参考文献
Kirai, Naohiro; Iguchi, Shoichiro; Ito, Tatsuyoshi; Takaya, Jun; Iwasawa, Nobuharu
Bulletin of the Chemical Society of Japan, 2013 , vol. 86, # 7 p. 784 - 799
反应条件
NaOC(CH3)3; methanol; CuCl(C3H4N2(C10H15)2) in tetrahydrofuran 5.0 molpercent Cu-complex, alkyne, diborane, 5.0 molpercent NaOC(CH3)3, 1.1 equiv CH3OH, THF, 22°C, 12 h, N2 atm.; 98:2 molar ratio of isomers;
参考文献
Jang, Hwanjong; Zhugralin, Adil R.; Lee, Yunmi; Hoveyda, Amir H.
Journal of the American Chemical Society, 2011 , vol. 133, # 20 p. 7859 - 7871
参考文献
Kalinin, Alexey V.; Scherer, Stefan; Snieckus, Victor
Angewandte Chemie - International Edition, 2003 , vol. 42, # 29 p. 3399 - 3404
反应条件
1: 4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl-4',4',5',5'-tetramethyl-1,3,2-dioxaborolane With cupric(II) carbonate; triphenylphosphine in water T=20°C; 0.5 h; Inert atmosphere; 2: 4-ethynyl-1-methoxy-benzene in water T=27°C; 24 h; Inert atmosphere;
参考文献
Stavber, Gaj; Casar, Zdenko
Applied Organometallic Chemistry, 2013 , vol. 27, # 3 p. 159 - 165
反应条件
ClRh(P(CH2CH2(CF2)5CF3)3)3 in further solvent(s) inert atmosphere; 40°C (12 h), cooling (room temp.); extg. (toluene), evapn. (vac.), chromy. (hexanes/ether=98:2); isolated as mixture of isomers, detd. by (1)H and (13)C NMR spectroscopy;
参考文献
Journal of the American Chemical Society, , vol. 121, # 12 p. 2696 - 2704
