N-乙酰基-N-苯基甘氨酸乙酯合成路线 (共 6 条)
反应条件
N,N,N',N'-tetramethyl-7,8-dihydro-6H-dipyrido[1,2-a;2',1'-c][1,4] diazepine-2,12-diamine in N,N-dimethyl-formamide T=20°C; 72 h; GloveboxUV-irradiation;
参考文献
O'Sullivan, Steven; Doni, Eswararao; Tuttle, Tell; Murphy, John A.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 2 p. 474 - 478
Angew. Chem., 2013 , vol. 126, # 2 p. 484 - 488,5
反应条件
sodium hydride in hexane; N,N-dimethyl-formamide; mineral oil
T=20°C; Inert atmosphere;
参考文献
O'Sullivan, Steven; Doni, Eswararao; Tuttle, Tell; Murphy, John A.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 2 p. 474 - 478
Angew. Chem., 2013 , vol. 126, # 2 p. 484 - 488,5
反应条件
sodium carbonate
Reflux;
参考文献
Pace, Vittorio; Holzer, Wolfgang; Verniest, Guido; Alcantara, Andres R.; De Kimpe, Norbert
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 5 p. 919 - 926
反应条件
hydrogenchloride; ethanol
参考文献
Paal; Otten
Chemische Berichte, 1890 , vol. 23, p. 2592
参考文献
Paal; Otten
Chemische Berichte, 1890 , vol. 23, p. 2592
反应条件
sodium hydroxide in ethanol; water
Heating;
参考文献
DeRuiter, Jack; Swearingen, Blake E.; Wandrekar, Vinay; Mayfield, Charles A.
Journal of Medicinal Chemistry, 1989 , vol. 32, # 5 p. 1033 - 1038