(3beta)-3-(甲酰氧基)-20-氧代孕甾-5-烯-17-基乙酸酯合成路线 (共 7 条)
反应条件
1: aluminium isopropylate; cyclohexanone; xylene 2: aqueous methanol.KOH View Scheme
参考文献
Ringold et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 820,823
反应条件
1: With aluminum isopropoxide in cyclohexanone; xylene 0.833333 h; distillation; 2: With water T=0°C;
参考文献
Boehringer Ingelheim International GmbH
Patent: EP1359154 A1, 2003 ;
Location in patent: Page/Page column 16; 28; 30; 32 ;
反应条件
1: With aluminum isopropoxide in cyclohexanone; xylene 0.833333 h; distillation; 2: With water T=0°C;
参考文献
Boehringer Ingelheim International GmbH
Patent: EP1359154 A1, 2003 ;
Location in patent: Page/Page column 16; 28; 30; 32 ;
反应条件
1: With aluminum isopropoxide in cyclohexanone; xylene 0.833333 h; distillation; 2: With water T=0°C;
参考文献
Boehringer Ingelheim International GmbH
Patent: EP1359154 A1, 2003 ;
Location in patent: Page/Page column 16; 28; 30; 32 ;
反应条件
1: methanol. KOH 2: chloroform; monoperoxyphthalic acid; diethyl ether View Scheme
参考文献
Bowers et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 5991
反应条件
1: methanol. KOH 2: chloroform; monoperoxyphthalic acid; diethyl ether 3: ether BF3 4: CrO3; acetone 5: HCl View Scheme
参考文献
Bowers et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 5991
参考文献
Bowers et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 5991