Mn(tetraphenylporphyrin) in acetonitrile-D3 T=25°C; 14 h; Inert atmosphere;
参考文献
Hull, Jonathan F.; Balcells, David; Sauer, Effiette L.O.; Raynaud, Christophe; Brudvig, Gary W.; Crabtree, Robert H.; Eisenstein, Odile
Journal of the American Chemical Society, 2010 , vol. 132, # 22 p. 7605 - 7616
in benzene Irradiation (UV/VIS); irrdn. for 2 h 40 min with a 450 W medium pressure mercury lamp (290 to 330 nm), under Ar; extn. (aq. NaOH), dried (Na2SO4), evapd., crystn. from hexane, yields 9,10-phenanthraquinone;
参考文献
de Vries, Johannes G.; Hubbard, Sally A.
Journal of the Chemical Society, Chemical Communications, 1988 , # 17 p. 1172 - 1173
in dichloromethane under Ar, at -79°C, allowed to warm up to room temp. and kept here overnight; half of the solvent stripped in vac., ether layered over the soln., standing, filtered, washed with ether, dried in vac., sepn. by washing with CH3CN; elem. anal.;
