2,3-二氯-5,6-二氰基-1,4-苯醌合成路线 (共 141 条)
反应条件
trimethylsilyl cyanide; lithium perchlorate in benzene
T=25°C; 0.25 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Sundberg, Richard J.; Theret, Marie-Helene; Wright, Lorna
Organic Preparations and Procedures International, 1994 , vol. 26, # 3 p. 386 - 389
反应条件
water in tetrahydrofuran
2 h; Ambient temperature;
参考文献
Yoshioka, Tadao; Mohri, Kunihiko; Oikawa, Yuji; Yonemitsu, Osamu
Journal of Chemical Research, Miniprint, 1981 , # 7 p. 2252 - 2281
反应条件
in tetrahydrofuran
Ambient temperature;
参考文献
Yoshioka, Tadao; Mohri, Kunihiko; Oikawa, Yuji; Yonemitsu, Osamu
Journal of Chemical Research, Miniprint, 1981 , # 7 p. 2252 - 2281
反应条件
copper diacetate; silver(l) oxide in 1-methyl-pyrrolidin-2-one
T=120°C; 20 h;
参考文献
Zheng, Kui; Yu, Peng; Chen, Shuyou; Chen, Fen; Cheng, Jiang
Chinese Journal of Chemistry, 2013 , vol. 31, # 4 p. 449 - 452
参考文献
BRISTOL-MYERS SQUIBB COMPANY
Patent: EP761666 A2, 1997 ;
反应条件
N,N,N-trimethylbenzenemethanaminium dichloroiodate in 1,4-dioxane
T=20°C; 2.5 h; Heating / reflux;
参考文献
Boehringer Ingelheim International GmbH
Patent: US2007/203125 A1, 2007 ;
Location in patent: Page/Page column 35 ;
反应条件
in 1,4-dioxane; hexane
参考文献
The Upjohn Company
Patent: US4459420 A1, 1984 ;
参考文献
Eisai Chemical Co., Ltd.
Patent: US5412124 A1, 1995 ;
反应条件
in acetone
T=25°C; other temperatures;
参考文献
Osawa, Yoshihiro; Nishimura, Norio; Yamamoto, Shunzo
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 9 p. 2648 - 2655
反应条件
in benzene
Ambient temperature;
参考文献
Nishida, Shinya; Murakami, Masashi; Oda, Hirofumi; Tsuji, Takashi; Mizuno, Tetsuo; et al.
Journal of Organic Chemistry, 1989 , vol. 54, # 16 p. 3859 - 3868