2,3-二氯-5,6-二氰基-1,4-苯醌合成路线 (共 141 条)
反应条件
copper diacetate; silver(l) oxide in 1-methyl-pyrrolidin-2-one T=120°C; 20 h;
参考文献
Zheng, Kui; Yu, Peng; Chen, Shuyou; Chen, Fen; Cheng, Jiang
Chinese Journal of Chemistry, 2013 , vol. 31, # 4 p. 449 - 452
反应条件
in hexane; ethyl acetate; toluene
参考文献
E. R. Squibb and Sons, Inc.
Patent: US5072023 A1, 1991 ;
参考文献
Glaxo Group Limited
Patent: US5037845 A1, 1991 ;
反应条件
copper diacetate; silver(l) oxide in 1-methyl-pyrrolidin-2-one T=120°C; 20 h;
参考文献
Zheng, Kui; Yu, Peng; Chen, Shuyou; Chen, Fen; Cheng, Jiang
Chinese Journal of Chemistry, 2013 , vol. 31, # 4 p. 449 - 452
反应条件
Ag2CO3; copper(II) bis(trifluoromethanesulfonate); potassium carbonate in N,N-dimethyl-formamide T=100°C; 20 h;
参考文献
Zhang, Guangyou; Chen, Shuyou; Fei, Haiyang; Cheng, Jiang; Chen, Fan
Synlett, 2012 , vol. 23, # 15 p. 2247 - 2250
反应条件
in acetonitrile T=25°C; Equilibrium constant;
参考文献
Iida, Yoichi
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 9 p. 2673 - 2674
反应条件
trimethylsilyl cyanide; lithium perchlorate in benzene T=80°C; 4 h;
参考文献
Sundberg, Richard J.; Theret, Marie-Helene; Wright, Lorna
Organic Preparations and Procedures International, 1994 , vol. 26, # 3 p. 386 - 389
反应条件
trimethylsilyl cyanide; lithium perchlorate in benzene-d6 T=25°C; 3 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Sundberg, Richard J.; Theret, Marie-Helene; Wright, Lorna
Organic Preparations and Procedures International, 1994 , vol. 26, # 3 p. 386 - 389
反应条件
in acetonitrile-D3 T=20°C; Inert atmosphere;
参考文献
Wang, Zheng-Lin; Li, Hong-Liang; Ge, Li-Shi; An, Xing-Lan; Zhang, Zi-Gang; Luo, Xiaoyan; Fossey, John S.; Deng, Wei-Ping
Journal of Organic Chemistry, 2014 , vol. 79, # 3 p. 1156 - 1165
反应条件
trimethylsilyl cyanide; lithium perchlorate in benzene T=25°C; 0.25 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Sundberg, Richard J.; Theret, Marie-Helene; Wright, Lorna
Organic Preparations and Procedures International, 1994 , vol. 26, # 3 p. 386 - 389