反应条件
1: Natriumhydrogenecarbonat / 0.5 h / 80 °C
2: 80 percent / PCl5 / 2 h
3: 1.) Na2SO3, Na2CO3, 2.) Tetrabutylammonium bromide / 1.) 5 min, reflux, water, 2.) 24 h, reflux, 1,2-dimethoxyethane
4: 1.) Thionylchlorid, 2.) Triethylamin / 1.) room temperature, CHCl3, 2.) room temperature, 24 h, benzene
View Scheme
参考文献
Horner, L.; Lindel, H.
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 15, p. 1 - 8
