Fmoc-N-甲基-L-丙氨酸合成路线 (共 7 条)
反应条件
triethylsilane; trifluoroacetic acid in chloroform
参考文献
Tetrahedron Letters, , vol. 52, # 30 p. 3872 - 3875
反应条件
trifluoroacetic acid in dichloromethane; toluene T=20°C; 1 h;
参考文献
Amino Acids, , vol. 38, # 1 p. 133 - 143
反应条件
1: N-methyl-N-nosyl-L-alanine phenacyl ester With benzenethiol sodium salt in N,N-dimethyl-formamide T=20°C; 3 h; Inert atmosphere; 2: With sodium carbonate in water pH=9; 3: (9H-Fluoren-9-yl)-methyl chloroformate in 1,4-dioxane T=0°C;
参考文献
Journal of Organic Chemistry, , vol. 75, # 5 p. 1386 - 1392
反应条件
1: toluene-4-sulfonic acid / toluene / 2 h / |Reflux 2: triethylsilane; trifluoroacetic acid / chloroform / 22 h / 20 °C View Scheme
参考文献
European Journal of Organic Chemistry, , # 21 p. 4509 - 4513
反应条件
Multistep reaction.;
参考文献
Journal of Organic Chemistry, , vol. 72, # 10 p. 3723 - 3728
反应条件
Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 38, # 42 p. 7307 - 7310
参考文献
Yang, Lihu; Morriello, Greg
Tetrahedron Letters, 1999 , vol. 40, # 47 p. 8197 - 8200