(5-溴-2-噻唑基)-亚氨基二羧酸二叔丁酯合成路线 (共 2 条)
反应条件
1: 5-bromo-thiazol-2-ylamine; hydrochloride With triethylamine in tetrahydrofuran
2: di-tert-butyl dicarbonate With 4-(N,N-dimethlyamino)pyridine in tetrahydrofuran
2 h; Heating / reflux;
参考文献
Genelabs Technologies, Inc.
Patent: US2007/265265 A1, 2007 ;
Location in patent: Page/Page column 105 ;
反应条件
4-(N,N-dimethlyamino)pyridine in tetrahydrofuran
Heating;
参考文献
Stanetty, Peter; Schnuerch, Michael; Mereiter, Kurt; Mihovilovic, Marko D.
Journal of Organic Chemistry, 2005 , vol. 70, # 2 p. 567 - 574