1: 85 percent / ethanol / 8 h / Ambient temperature
2: 90 percent / triethylamine / methanol / 2 h / Ambient temperature
3: 94 percent / silica gel / CHCl3 / 5 h / Heating
View Scheme
参考文献
Joshi, S. D.; Usgaonkar, R. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 5 p. 399 - 402
1: 0.4 g / NaBH4 / methanol / 0.5 h / T < 40 deg C
2: 0.45 g / PCl5 / benzene / 4 h / Heating
View Scheme
参考文献
Joshi, S. D.; Usgaonkar, R. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 5 p. 399 - 402