4,5,6,7-四氢苯并呋喃-4-醇合成路线 （共 9 条）
反应条件
in toluene T=-75°C; Paterno-Buechi reaction; 6 h; UV-irradiation; Further byproducts.;
参考文献
Yabuno, Youhei; Hiraga, Yoshikazu; Abe, Manabu
Chemistry Letters, 2008 , vol. 37, # 8 p. 822 - 823
反应条件
in toluene T=60°C; Paterno-Buechi reaction; 6 h; UV-irradiation; Further byproducts.;
参考文献
Yabuno, Youhei; Hiraga, Yoshikazu; Abe, Manabu
Chemistry Letters, 2008 , vol. 37, # 8 p. 822 - 823
反应条件
in toluene T=60°C; Paterno-Buechi reaction; 6 h; UV-irradiation; Further byproducts.;
参考文献
Chemistry Letters, , vol. 37, # 8 p. 822 - 823
反应条件
sodium tetrahydroborate in methanol
0.5 h; Ambient temperature;
参考文献
Tada; Ohtsu; Chiba
Chemical and Pharmaceutical Bulletin, 1994 , vol. 42, # 10 p. 2167 - 2169
反应条件
potassium hydride in tetrahydrofuran
T=25°C; 16 h;
参考文献
Cohen; Bhupathy; Matz
Journal of the American Chemical Society, 1983 , vol. 105, # 3 p. 520 - 525
反应条件
iron(II) sulfate in tetrahydrofuran; water
参考文献
Herz, Werner; Juo, Rouh-Rong
Journal of Organic Chemistry, 1985 , vol. 50, # 5 p. 618 - 627
反应条件
1: 96 percent / LiAlH4 / diethyl ether
2: 33 percent / KH / tetrahydrofuran / 16 h / 25 °C
View Scheme
参考文献
Cohen; Bhupathy; Matz
Journal of the American Chemical Society, 1983 , vol. 105, # 3 p. 520 - 525
反应条件
1: 1.) aq. NaHCO3, 2.) aq. H2SO4
2: 89 percent / NaBH4 / methanol / 2 h / Ambient temperature
View Scheme
参考文献
Lee, Mase; Moritomo, Hiroyuki; Kanematsu, Ken
Tetrahedron, 1996 , vol. 52, # 24 p. 8169 - 8180
反应条件
1:
2: With lithium aluminium tetrahydride
参考文献
Iida, Kazunori; Mitani, Makoto; Kuroda, Chiaki
Bulletin of the Chemical Society of Japan, 2007 , vol. 80, # 5 p. 966 - 971
