2,3,3-三甲基-3H-吲哚-5-羧酸合成路线 （共 7 条）
反应条件
sulfuric acid in ethanol 12 h; Heating;
参考文献
Tomasulo, Massimiliano; Kaanumal, Sireesha L.; Sortino, Salvatore; Raymo, Francisco M.
Journal of Organic Chemistry, 2007 , vol. 72, # 2 p. 595 - 605
反应条件
in acetic acid 12 h; Reflux;
参考文献
Oushiki, Daihi; Kojima, Hirotatsu; Terai, Takuya; Arita, Makoto; Hanaoka, Kenjiro; Urano, Yasuteru; Nagano, Tetsuo
Journal of the American Chemical Society, 2010 , vol. 132, # 8 p. 2795 - 2801
反应条件
in acetic acid 3.5 h; Heating;
参考文献
Lindsey, Jonathan S.; Brown, Philip A.; Siesel, David A.
Tetrahedron, 1989 , vol. 45, # 15 p. 4845 - 4866
反应条件
1.1: conc. hydrochloric acid; sodium nitrite / H2O / 0.5 h / 0 °C 1.2: conc. hydrochloric acid; stannous chloride dihydrate / H2O / 0.5 h / 0 °C 2.1: conc. sulfuric acid / ethanol / 7 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 39, # 1 p. 179 - 184
反应条件
1: ethanol / 4 h / |Reflux 2: acetic acid / 4 h / |Reflux View Scheme
参考文献
ChemSusChem, , vol. 6, # 1 p. 70 - 77
反应条件
1: ethanol / 4 h / |Reflux 2: acetic acid / 4 h / |Reflux View Scheme
参考文献
ChemSusChem, , vol. 6, # 1 p. 70 - 77
反应条件
dicyclohexyl-carbodiimide in DMF (N,N-dimethyl-formamide) T=20°C;
参考文献
Stavrianopoulos, Jannis G.; Rabbani, Elazar
Patent: US2003/225247 A1, 2003 ;
Location in patent: Page 32 ;
