N-[3-烯丙基-4-羟基苯基]乙酰胺合成路线 （共 10 条）
参考文献
Claisen
Justus Liebigs Annalen der Chemie, 1919 , vol. 418, p. 102
反应条件
potassium carbonate in diphenylether; butanone
参考文献
Zeneca Limited
Patent: US5866611 A1, 1999 ;
反应条件
1: ammonium sulfide
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参考文献
Jacobs; Heidelberger
Journal of the American Chemical Society, 1917 , vol. 39, p. 2190
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Claisen
Justus Liebigs Annalen der Chemie, 1919 , vol. 418, p. 102
反应条件
1: petroleum
View Scheme
参考文献
Claisen
Justus Liebigs Annalen der Chemie, 1919 , vol. 418, p. 102
参考文献
Jacobs; Heidelberger
Journal of the American Chemical Society, 1917 , vol. 39, p. 2190
Full Text Show Details
Claisen
Justus Liebigs Annalen der Chemie, 1919 , vol. 418, p. 102
反应条件
1: potassium carbonate / acetone / 16 h / |Reflux
2: SnCl2·2H2O / ethanol / 0.33 h / |Reflux; |Inert atmosphere
3: chloroformic acid ethyl ester; triethylamine / chloroform / 0.75 h / 20 - 50 °C
4: N,N-diethylaniline; hydrogen / 6 h / 200 °C
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参考文献
Jabbari, Atena; Davoodnejad, Mahdieh; Alimardani, Maliheh; Assadieskandar, Amir; Sadeghian, Ali; Safdari, Hadi; Movaffagh, Jebraeel; Sadeghian, Hamid
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 18 p. 5518 - 5526
反应条件
1: SnCl2·2H2O / ethanol / 0.33 h / |Reflux; |Inert atmosphere
2: chloroformic acid ethyl ester; triethylamine / chloroform / 0.75 h / 20 - 50 °C
3: N,N-diethylaniline; hydrogen / 6 h / 200 °C
View Scheme
参考文献
Jabbari, Atena; Davoodnejad, Mahdieh; Alimardani, Maliheh; Assadieskandar, Amir; Sadeghian, Ali; Safdari, Hadi; Movaffagh, Jebraeel; Sadeghian, Hamid
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 18 p. 5518 - 5526
反应条件
1: potassium carbonate; acetone
2: sulfuric acid
3: petroleum
View Scheme
参考文献
Claisen
Justus Liebigs Annalen der Chemie, 1919 , vol. 418, p. 102
反应条件
T=181°C; Rate constant;
参考文献
White et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 3271,3272
参考文献
Claisen
Justus Liebigs Annalen der Chemie, 1919 , vol. 418, p. 102
