(9CI)-1,2,3,4-四氢-6-甲基吡啶并[1,2-a]苯并咪唑合成路线 （共 7 条）
反应条件
1: 48 percent / hydrogen peroxide (30 percent) / acetic acid / 3 h / 90 °C
2: 68.3 percent / propan-1-ol / 150 h / Heating
3: H2 / Raney nickel / ethanol
4: hydrogen peroxide / trifluoroacetic acid
View Scheme
参考文献
Piotrovskii, L.B.; Poznyakova, L.N.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 1691 - 1695
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 9 p. 1931 - 1935
反应条件
1: 68.3 percent / propan-1-ol / 150 h / Heating
2: H2 / Raney nickel / ethanol
3: hydrogen peroxide / trifluoroacetic acid
View Scheme
参考文献
Piotrovskii, L.B.; Poznyakova, L.N.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 1691 - 1695
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 9 p. 1931 - 1935
反应条件
1: H2 / Raney nickel / ethanol
2: hydrogen peroxide / trifluoroacetic acid
View Scheme
参考文献
Piotrovskii, L.B.; Poznyakova, L.N.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 1691 - 1695
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 9 p. 1931 - 1935
反应条件
1: 95 percent / 4 M HCl / 1 h / Heating
2: 97 percent / SOCl2 / 1 h / 80 °C
3: 0.0084 g / NaH / ethanol; paraffin / 30 °C
View Scheme
参考文献
Haque, M. Rezaul; Rasmussen, Malcolm
Tetrahedron, 1997 , vol. 53, # 20 p. 6937 - 6958
反应条件
1: 97 percent / SOCl2 / 1 h / 80 °C
2: 0.0084 g / NaH / ethanol; paraffin / 30 °C
View Scheme
参考文献
Haque, M. Rezaul; Rasmussen, Malcolm
Tetrahedron, 1997 , vol. 53, # 20 p. 6937 - 6958
反应条件
1: 95 percent / 4 M HCl / 1 h / Heating
2: 97 percent / SOCl2 / 1 h / 80 °C
3: 0.0084 g / NaH / ethanol; paraffin / 30 °C
View Scheme
参考文献
Haque, M. Rezaul; Rasmussen, Malcolm
Tetrahedron, 1997 , vol. 53, # 20 p. 6937 - 6958
反应条件
dihydrogen peroxide in trifluoroacetic acid
Yield given;
参考文献
Piotrovskii, L.B.; Poznyakova, L.N.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 1691 - 1695
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 9 p. 1931 - 1935
