4-苯亚甲基-2-苯基-5(4H)-恶唑酮合成路线 (共 45 条)
反应条件
iron(III) oxide; acetic anhydride T=25 - 30°C; Erlenmeyer-Plochl-Bergmann; 0.166667 h; SonicationIrradiation;
参考文献
Ahmadi, Seyed Javad; Sadjadi, Sodeh; Hosseinpour, Morteza
Ultrasonics Sonochemistry, 2013 , vol. 20, # 1 p. 408 - 412
反应条件
aluminum oxide in chloroform T=20°C; Perkin condensation;
参考文献
Conway, Philip A.; Devine, Kevin; Paradisi, Francesca
Tetrahedron, 2009 , vol. 65, # 15 p. 2935 - 2938
反应条件
trichlorophosphate in acetonitrile 0.333333 h; Heating;
参考文献
Khosropour, Ahmad R.; Khodaei, Mohammad M.; Hoseini Jomor, Seyed J.
Journal of Heterocyclic Chemistry, 2008 , vol. 45, # 3 p. 683 - 686
反应条件
1: benzyl alcohol With di[1,6-bis(3-methylimidazolium-1-yl)hexane]decatungstate; [bmim+][NO3-] T=80°C; 2: N-(benzoyl)glycine With acetic anhydride T=80°C; Erlenmeyer-Plochl azlactone and amino acid synthesis;
参考文献
Rostami, Mahboubeh; Khosropour, Ahmad Reza; Mirkhani, Valiollah; Mohammadpoor-Baltork, Iraj; Moghadam, Majid; Tangestaninejad, Shahram
Monatshefte fur Chemie, 2011 , vol. 142, # 11 p. 1175 - 1180
反应条件
tert-butylhypochlorite; potassium carbonate in tetrachloromethane 1) RT, 16 h; 2) reflux, 6.5 h;
参考文献
Lott, Richard S.; Breitholle, Edward G.; Stammer, Charles H.
Journal of Organic Chemistry, 1980 , vol. 45, # 6 p. 1151 - 1153
反应条件
1: DCC / tetrahydrofuran / 2 h / Ambient temperature 2: triethylamine / dioxane / 1 h 3: Dichlorodicyano-p-benzoquinone (DDQ), disilylacetamide / dioxane / 1 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 45, # 6 p. 1151 - 1153
反应条件
sodium acetate; acetic anhydride 0.05 h; Heating;
参考文献
Abdel-Motaleb, Ramadan M.; Bakeer, Hadeer M.; Tamam, Gammal H.; Arafa, Wael A. A.
Journal of Heterocyclic Chemistry, 2012 , vol. 49, # 5 p. 1071 - 1076,6
反应条件
thionyl chloride T=38°C; 96 h;
参考文献
Journal of Organic Chemistry, , vol. 34, # 6 p. 1621 - 1627
反应条件
bis-silyl acetamide; 2,3-dicyano-5,6-dichloro-p-benzoquinone in 1,4-dioxane 1 h; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 45, # 6 p. 1151 - 1153
反应条件
in benzene 0.166667 h; Heating;
参考文献
Kumar, Pradeep; Mukerjee, Arya K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 5 p. 418 - 420