1-溴-4-氟-2-(甲氧基甲基)苯合成路线 （共 3 条）
反应条件
1: triethylamine; palladium diacetate; 1,3-bis-(diphenylphosphino)propane / dimethyl sulfoxide 2: sulfuric acid; potassium nitrate / 4.5 h / -10 °C View Scheme
反应条件
sodium hydride in tetrahydrofuran
T=0 - 20°C;
参考文献
Ikeuchi, Yutaka; Taguchi, Takeo; Hanzawa, Yuji
Journal of Organic Chemistry, 2005 , vol. 70, # 2 p. 756 - 759
反应条件
1: 99 percent / DIBAL / tetrahydrofuran; hexane / 2.5 h / 0 °C
2: 100 percent / NaH / tetrahydrofuran / 0 - 20 °C
View Scheme
参考文献
Ikeuchi, Yutaka; Taguchi, Takeo; Hanzawa, Yuji
Journal of Organic Chemistry, 2005 , vol. 70, # 2 p. 756 - 759
