Paul, Rolf; Brockman, John A.; Hallett, W. A.; Hanifin, John W.; Tarrant, M. Ernestine; et al.
Journal of Medicinal Chemistry, 1985 , vol. 28, # 11 p. 1704 - 1716
1: 54 percent / tetrahydrofuran; diethyl ether / 3.5 h / Ambient temperature
2: 78 percent / CrO3, H2SO4 / H2O; acetone / 0.5 h / Ambient temperature
View Scheme
参考文献
Paul, Rolf; Brockman, John A.; Hallett, W. A.; Hanifin, John W.; Tarrant, M. Ernestine; et al.
Journal of Medicinal Chemistry, 1985 , vol. 28, # 11 p. 1704 - 1716
acetic acid
1.) butanol, reflux, 5 h, 2.) diphenyl ether, from 206 deg C to 217 deg C, 30 min; Yield given. Multistep reaction;
参考文献
Paul, Rolf; Brockman, John A.; Hallett, W. A.; Hanifin, John W.; Tarrant, M. Ernestine; et al.
Journal of Medicinal Chemistry, 1985 , vol. 28, # 11 p. 1704 - 1716
