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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
84233-60-3
合成路线
（共 8 条）
84233-60-3
→
反应条件
115274-33-4
反应条件
1: 78 percent / K2CO3 / dimethylformamide / 5 h / 80 °C 2: 30 percent / 1.) 20 percent HCl, 2.) NH4OH / 4 h / Heating View Scheme
参考文献
Nishimura; Minamida; Matsumoto -i.
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, # 3 p. 1223 - 1228
84233-60-3
→
反应条件
74274-64-9
反应条件
1: 89.7 percent / K2CO3 / dimethylformamide / 3 h / 100 °C 2: 82 percent / 20percent NaOH / 43 h / Heating 3: 91.4 percent / POCl3 / 0.25 h / Heating 4: 79.6 percent / acetonitrile / 1 h / Heating View Scheme
参考文献
Matsumoto; Miyamoto; Minamida; Nishimura; Egawa
Journal of Medicinal Chemistry, 1984 , vol. 27, # 3 p. 292 - 301
84233-60-3
→
反应条件
74274-67-2
反应条件
1: 89.7 percent / K2CO3 / dimethylformamide / 3 h / 100 °C 2: 82 percent / 20percent NaOH / 43 h / Heating 3: 91.4 percent / POCl3 / 0.25 h / Heating 4: 91.6 percent / acetonitrile / 1 h / Heating View Scheme
参考文献
Matsumoto; Miyamoto; Minamida; Nishimura; Egawa
Journal of Medicinal Chemistry, 1984 , vol. 27, # 3 p. 292 - 301
84233-60-3
→
反应条件
74274-70-7
反应条件
1: 89.7 percent / K2CO3 / dimethylformamide / 3 h / 100 °C 2: 82 percent / 20percent NaOH / 43 h / Heating 3: 91.4 percent / POCl3 / 0.25 h / Heating 4: 31.7 percent / acetonitrile / 1 h / Heating View Scheme
参考文献
Matsumoto; Miyamoto; Minamida; Nishimura; Egawa
Journal of Medicinal Chemistry, 1984 , vol. 27, # 3 p. 292 - 301
84233-60-3
→
反应条件
74274-71-8
1-乙烯基-6-氟-4-氧代-7-哌嗪-1-基-1,8-萘啶-3-羧酸
反应条件
1: 92.9 percent / K2CO3 / dimethylformamide / 3 h / 100 °C 2: 90.3 percent / SOCl2 / CHCl3 / 0.5 h / Heating 3: 80.6 percent / KOH / ethanol / 2 h / Heating 4: 82.4 percent / 10percent NaOH / 2 h / Heating View Scheme
参考文献
Matsumoto; Miyamoto; Minamida; Nishimura; Egawa
Journal of Medicinal Chemistry, 1984 , vol. 27, # 3 p. 292 - 301
84233-60-3
→
反应条件
74274-72-9
反应条件
1: 92.9 percent / K2CO3 / dimethylformamide / 3 h / 100 °C 2: 90.3 percent / SOCl2 / CHCl3 / 0.5 h / Heating 3: 80.6 percent / KOH / ethanol / 2 h / Heating 4: 82.4 percent / 10percent NaOH / 2 h / Heating 5: 43.6 percent / HCO2H / H2O / 17 h / 120 - 125 °C View Scheme
参考文献
Matsumoto; Miyamoto; Minamida; Nishimura; Egawa
Journal of Medicinal Chemistry, 1984 , vol. 27, # 3 p. 292 - 301
84233-60-3
→
反应条件
87939-12-6
1-乙基-6-氟-4-氧代-7-(3-氧代-1-哌嗪基)-1,4-二氢-1,8-萘啶-3-羧酸
反应条件
1: 89.7 percent / K2CO3 / dimethylformamide / 3 h / 100 °C 2: 82 percent / 20percent NaOH / 43 h / Heating 3: 91.4 percent / POCl3 / 0.25 h / Heating 4: 71.4 percent / acetonitrile / 1 h / Heating View Scheme
参考文献
Matsumoto; Miyamoto; Minamida; Nishimura; Egawa
Journal of Medicinal Chemistry, 1984 , vol. 27, # 3 p. 292 - 301
84233-60-3
→
反应条件
79286-73-0
反应条件
1: 89.7 percent / K2CO3 / dimethylformamide / 3 h / 100 °C 2: 82 percent / 20percent NaOH / 43 h / Heating 3: 91.4 percent / POCl3 / 0.25 h / Heating View Scheme
参考文献
Matsumoto; Miyamoto; Minamida; Nishimura; Egawa
Journal of Medicinal Chemistry, 1984 , vol. 27, # 3 p. 292 - 301
