反应条件
1: 1.) Mg, 2.) Et2NPOCl2, 3.) aq. HCl (d 1.18) / 1) diethyl ether, 45min, THF, reflux, 2 h; 2) diethyl ether, reflux, 1 h3) 110 deg C, 5 h
2: hydriodic acid (d 1.7) / 0.33 h / Heating
View Scheme
参考文献
Cornforth, John; Sierakowski, Andrew F.; Wallace Timothy W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 10 p. 2299 - 2316
