2-叠氮-D-半乳糖四乙酸酯合成路线 （共 14 条）
反应条件
1: D-Galactosamine hydrochloride With potassium carbonate; copper(II) sulfate in methanol T=20°C; 2 h; 2: acetic anhydride With pyridine 3 h; Further stages.;
参考文献
Goddard-Borger, Ethan D.; Stick, Robert V.
Organic Letters, 2007 , vol. 9, # 19 p. 3797 - 3800
反应条件
1: trifluoromethanesulfonyl azide; copper(II) sulfate; potassium carbonate / CH2Cl2; H2O; methanol / 16 h 2: pyridine / 2 h View Scheme
参考文献
Journal of Carbohydrate Chemistry, , vol. 24, # 4-6 p. 463 - 474
反应条件
sodium acetate in (2S)-N-methyl-1-phenylpropan-2-amine hydrate; acetic acid
反应条件
pyridine T=0°C; 4 h; Yield given;
参考文献
Helvetica Chimica Acta, , vol. 74, # 8 p. 2073 - 2077
反应条件
pyridine T=20°C; 15 h;
参考文献
Guazzelli, Lorenzo; Catelani, Giorgio; D'Andrea, Felicia; Giannarelli, Alessia
Carbohydrate Research, 2009 , vol. 344, # 3 p. 298 - 303
反应条件
in tetrachloromethane T=0°C; 1 h; Irradiation;
参考文献
Carbohydrate Research, , vol. 98, p. 25 - 36
反应条件
1: imidazole-1-sulfonyl azide hydrochloride; potassium carbonate; copper(II) sulfate / methanol / 20 °C 2: pyridine View Scheme
参考文献
Organic Letters, , vol. 15, # 19 p. 5060 - 5063
反应条件
in tetrachloromethane T=0°C; 2 h; Irradiation;
参考文献
Carbohydrate Research, , vol. 98, p. 25 - 36
反应条件
azido chloride in tetrachloromethane T=0°C; 1 h; Irradiationother halogen-azide, in other solvents under irradiation or in the dark, various time; Product distribution;
参考文献
Carbohydrate Research, , vol. 98, p. 25 - 36
参考文献
Ahad, Ali M.; Jensen, Stephanie M.; Jewett, John C.
Organic Letters, 2013 , vol. 15, # 19 p. 5060 - 5063
