(+)-2-O-苄基-l-苏丁醇合成路线 (共 2 条)
反应条件
1: H2 / 10percent Pd-C / ethanol 2: NaHCO3, NaIO4 / H2O / 0.25 h / Ambient temperature View Scheme
参考文献
Tanaka, Akira; Otsuka, Soichiro; Yamashita, Kyohei
Agricultural and Biological Chemistry, 1984 , vol. 48, # 8 p. 2135 - 2136
反应条件
1: 85 percent / H2 / palladium black / ethanol / 2 h / Ambient temperature 2: 1.) Pb(OAc)4; 2.) NaBH4 / 1.) ethyl acetate, benzene, 50 deg C, 1 h; 2.) ethanol, room temp., 5 h View Scheme
参考文献
Al-Hakim, Ali; Haines, Alan H.; Morley, Christopher
Synthesis, 1985 , # 2 p. 207 - 208