呋喃并[2,3-c]吡啶-7(6h)-酮合成路线 （共 5 条）
反应条件
1: With triethylamine in acetone T=0°C; 0.666667 h; 2: With sodium azide in water; acetone T=0°C; 1 h; 3: With tributyl-amine in diphenyl Methane; benzene T=220°C; 1.5 h;
参考文献
ASKA Pharmaceutical Co., Ltd.
Patent: EP1724267 A1, 2006 ;
Location in patent: Page/Page column 128 ;
反应条件
tributyl-amine in various solvent(s) T=175 - 185°C;
参考文献
Shiotani, Shunsaku; Morita, Hiroyuki
Journal of Heterocyclic Chemistry, 1982 , vol. 19, p. 1207 - 1209
反应条件
1: With triethylamine in acetone Cooling with ice; 2: With sodium azide in water; acetone 1 h; Cooling with ice; 3: With tributyl-amine; diphenylamine T=220°C; 1.5 h;
参考文献
Asagarasu, Akira; Matsui, Teruaki; Hayashi, Hiroyuki; Tamaoki, Satoru; Yamauchi, Yukinao; Sato, Michitaka
Chemical and Pharmaceutical Bulletin, 2009 , vol. 57, # 1 p. 34 - 42
反应条件
1: 85.6 percent / phosphorus oxychloride / 3 h / Heating 2: 95.5 percent / powdered zinc / acetic acid / 5 h / Heating View Scheme
参考文献
Shiotani, Shunsaku; Morita, Hiroyuki
Journal of Heterocyclic Chemistry, 1982 , vol. 19, p. 1207 - 1209
反应条件
trichlorophosphate 3 h; Heating;
参考文献
Shiotani, Shunsaku; Morita, Hiroyuki
Journal of Heterocyclic Chemistry, 1982 , vol. 19, p. 1207 - 1209
